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Grenoble INP
EQUIPMENTS
EQUIPMENTS
EQUIPMENTS
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Laboratory equipments

THERMAL ANALYSIS


· Thermogravimetric analysis, TGA 1000°C (METTLER-TOLEDO, LF1100-XP1)

· Thermogravimetric analysis, TGA-TD 1600°C (SETARAM, TAG24)

· Differential Scanning Calorimetry, DSC -150/500°C (METTLER-TOLEDO, DSC1/500/2412)

· Differential Scanning Calorimetry, 300°C/1000b (SETARAM, C80)

TEXTURAL ANALYSIS - PHYSICAL PROPERTIES


· Surface Area and Porosimetry Analyzer (MICROMERITICS, ASAP 2020)

· Particle sizing (Laser light scattering) : 10nm / 2.1mm, (MALVERN, Mastersizer 3000)

· Zetameter (zeta potentiel / particle sizing : 2nm/2um), (MALVERN, Zetasizer 3000HS)

· Scanning tunneling microscope, STM (AGILENT, 5100 AFM)

· Viscosimeter (TA INSTRUMENTS, DHR-3 rheometer)

· Dynamic Mechanical Analysis, DMA (TA INSTRUMENTS, Q800)

· Dilatometer (NETZSCH, DIL 402C)

· Capillary viscometer (SCHOTT, AVS-360)

· Fusion point <400°C, (SCHORPP, APA II)

CHROMATOGRAPHY


· Size exclusion chromatography, SEC (WATERS)

· Size exclusion chromatography / multiangle laser light scattering, SEC-MALLS (WATERS / SOPARES / WYATT)

· Flash chromatography (GRACE, Reveleris flash system)

· Ion chromatography (METROHM, 881 Compact IC PRO)

· High-performance liquid chromatography, HPLC-UV-RI (AGILENT TECHNOLOGIES, 1260 Infinity)

· Gas chromatography, CPV-TCD-FID (HEWLETT-PACKARD, 6890)

SPECTROSCOPY


· Raman spectrometer, 229/244/363/514/488/647nm (JOBIN-YVON T64000)

· Raman spectrometer, 514nm (RENISHAW, InVia RM 1000)

· Raman spectrometer, 514/785nm (RENISHAW, Invia)

· UV spectrometer, 190/1100nm (SHIMADZU, UV-2501PC / JASCO V-530)

· IRTF spectrometer, 50-7000cm-1 (BRUKER, VERTEX 70V)

. NMR Spectroscopy, 400MHz, BBO + MICZ5574/0015, Pulse Field Gradient (PFG) NMR, 117 Gauss/cm/A, Diffusion coefficients determination, (BRUKER, Avance III HD)

ELECTROCHEMISTRY


· Potentiostats (AUTOLAB, SOLARTRON, BIOLOGIC, AMETECH, BIORITECH GAMRY, RADIOMETER…)

· Proton exchange membrane fuel cell, PEMFC (PAXITECH BIOLOGIC, FCT-50S)

· Conductivimeter, tree electrodes (M2E)

· Differential Electrochemical Mass Spectrometry, DEMS (LEPMI / PFEIFFER)

· Oxygen semi-permeability (M2E)

· High temperature electrolysis (EHT)

· Solid oxide fuel cells, SOFC (LEPMI)

SYNTHESYS


· Current sintering bench, 5s/900°C (M2E)

· Furnace <1750°C (CARBOLITE, PYROX, NABERTHERM…)

· Furnace <3000°C (NABERTHERM, BOUHWIK)

DEPOSITION


· Electrospray deposition 20KV, ESD 80mm / ESD150mm (LEPMI / ALPES INSTRUMENT)

· Sputtering (EMITECH, SC7620)

· Serigraphie, 350x400mm, (JFP MICROTECHNIC, AUREL C900)

· Spray coating (IAI, Tabletop TT)

· Chemical vapor deposition, Pyrosol 800KHz (LEPMI / RBI)

CONDITIONNING


· Automatic Film Applicator (ELCOMETER, 4340)

· Polishing (MECAPOL, P200)

· Freeze Dryer, -110°C (THERMO ELECTRON CORPORATION, Heto PowerDry LL1500)

· Isostatic pressing, 3000bars (ALSTHOM ATLANTIQUE)

· Uniaxial pressing, 5T (PAUL WEBER)

· Planetary Micro Mill, (FRITSCH, Pulverisette 7)

· Sieving (RETSCH, AS200)

· Tridimensionnal mixer (TURBULA de WAB)

· Attritor (NETZSCH)

· Atomisor (BUCHI, Minispray Dryer B-290)

· Roller mixer (EXAKT)

· Distillator (WATER STILL, Distinction D4000)

· Centrifuge, 15000tr/min (HETTICH-ZENTRIFUGEN, Universal 320R / SIGMA, 3-10)

OTHER


· Karl Fisher method (TITROLINE, 7500 KF)

· Pump system / Oxygen gauge (LEPMI)

· Abbe refractometer, 1,30000 à 1.71000 ±0.0001 (ATAGO, 3T)

Written by Olivier Szydlo

Date of update May 27, 2016

Communauté Université Grenoble Alpes