LEPMI - Rubrique Equipements

Laboratory equipments

Thermal analysis

  • Thermogravimetric analysis, TGA 1000°C (METTLER-TOLEDO, LF1100-XP1)
  • Thermogravimetric analysis, TGA-TD 1600°C (SETARAM, TAG24)
  • Differential Scanning Calorimetry, DSC -150/500°C (METTLER-TOLEDO, DSC1/500/2412)
  • Differential Scanning Calorimetry, 300°C/1000b (SETARAM, C80)

Textural analysis - Physical properties

  • Surface Area and Porosimetry Analyzer (MICROMERITICS, ASAP 2020)
  • Particle sizing (Laser light scattering) : 10nm / 2.1mm, (MALVERN, Mastersizer 3000)
  • Zetameter (zeta potentiel / particle sizing : 2nm/2um), (MALVERN, Zetasizer 3000HS)
  • Scanning tunneling microscope, STM (AGILENT, 5100 AFM)
  • Viscosimeter (TA INSTRUMENTS, DHR-3 rheometer)
  • Dynamic Mechanical Analysis, DMA (TA INSTRUMENTS, Q800)
  • Dilatometer (NETZSCH, DIL 402C)
  • Capillary viscometer (SCHOTT, AVS-360)
  • Fusion point <400°C, (SCHORPP, APA II)

Chromatography

  • Size exclusion chromatography, SEC (WATERS)
  • Size exclusion chromatography / multiangle laser light scattering, SEC-MALLS (WATERS / SOPARES / WYATT)
  • Flash chromatography (GRACE, Reveleris flash system)
  • Ion chromatography (METROHM, 881 Compact IC PRO)
  • High-performance liquid chromatography, HPLC-UV-RI (AGILENT TECHNOLOGIES, 1260 Infinity)
  • Gas chromatography, CPV-TCD-FID (HEWLETT-PACKARD, 6890)

Spectroscopy

  • Raman spectrometer, 229/244/363/514/488/647nm (JOBIN-YVON T64000)
  • Raman spectrometer, 514nm (RENISHAW, InVia RM 1000)
  • Raman spectrometer, 514/785nm (RENISHAW, Invia)
  • UV spectrometer, 190/1100nm (SHIMADZU, UV-2501PC / JASCO V-530)
  • IRTF spectrometer, 50-7000cm-1 (BRUKER, VERTEX 70V)
  • NMR Spectroscopy, 400MHz, BBO + MICZ5574/0015, Pulse Field Gradient (PFG) NMR, 117 Gauss/cm/A, Diffusion coefficients determination, (BRUKER, Avance III HD)

Electrochemistry

  • Potentiostats (AUTOLAB, SOLARTRON, BIOLOGIC, AMETECH, BIORITECH GAMRY, RADIOMETER…)
  • Proton exchange membrane fuel cell, PEMFC (PAXITECH BIOLOGIC, FCT-50S)
  • Conductivimeter, tree electrodes (M2E)
  • Differential Electrochemical Mass Spectrometry, DEMS (LEPMI / PFEIFFER)
  • Oxygen semi-permeability (M2E)
  • High temperature electrolysis (EHT)
  • Solid oxide fuel cells, SOFC (LEPMI)

Synthesys

  • Current sintering bench, 5s/900°C (M2E)
  • Furnace <1750°C (CARBOLITE, PYROX, NABERTHERM…)
  • Furnace <3000°C (NABERTHERM, BOUHWIK)

Deposition

  • Electrospray deposition 20KV, ESD 80mm / ESD150mm (LEPMI / ALPES INSTRUMENT)
  • Sputtering (EMITECH, SC7620)
  • Serigraphie, 350x400mm, (JFP MICROTECHNIC, AUREL C900)
  • Spray coating (IAI, Tabletop TT)
  • Chemical vapor deposition, Pyrosol 800KHz (LEPMI / RBI)

Conditionning

  • Automatic Film Applicator (ELCOMETER, 4340)
  • Polishing (MECAPOL, P200)
  • Freeze Dryer, -110°C (THERMO ELECTRON CORPORATION, Heto PowerDry LL1500)
  • Isostatic pressing, 3000bars (ALSTHOM ATLANTIQUE)
  • Uniaxial pressing, 5T (PAUL WEBER)
  • Planetary Micro Mill, (FRITSCH, Pulverisette 7)
  • Sieving (RETSCH, AS200)
  • Tridimensionnal mixer (TURBULA de WAB)
  • Attritor (NETZSCH)
  • Atomisor (BUCHI, Minispray Dryer B-290)
  • Roller mixer (EXAKT)
  • Distillator (WATER STILL, Distinction D4000)
  • Centrifuge, 15000tr/min (HETTICH-ZENTRIFUGEN, Universal 320R / SIGMA, 3-10)

Other

  • Karl Fisher method (TITROLINE, 7500 KF)
  • Pump system / Oxygen gauge (LEPMI)
  • Abbe refractometer, 1,30000 à 1.71000 ±0.0001 (ATAGO, 3T)